| Identification | Back Directory | [Name]
4-Hydrazinylpyridin-2(1H)-one | [CAS]
106689-41-2 | [Synonyms]
4-Hydrazinylpyridin-2(1H)
4-Hydrazino-1H-Pyridin-2-One
4-Hydrazinyl-1H-pyridin-2-one
4-hydrazinylpyridin-2(1H)-one
4-Hydrazinyl-2(1H)-pyridinone
2(1H)-PYRIDINONE, 4-HYDRAZINO-
2(1H)-Pyridinone, 4-hydrazinyl-
2(1H)-Pyridinone,4-hydrazino-(9CI) | [Molecular Formula]
C5H7N3O | [MDL Number]
MFCD18071580 | [MOL File]
106689-41-2.mol | [Molecular Weight]
125.13 |
| Chemical Properties | Back Directory | [Melting point ]
245 °C | [Boiling point ]
393.2±42.0 °C(Predicted) | [density ]
1.30±0.1 g/cm3(Predicted) | [storage temp. ]
Inert atmosphere,Store in freezer, under -20°C | [pka]
11.56±0.10(Predicted) | [Appearance]
White to yellow Solid |
| Hazard Information | Back Directory | [Synthesis]
Step 1: 2,4-Dihydroxypyridine (20.3 g, 183.0 mmol) was added to a mixed solution of 2-methoxyethanol (400 mL) and 55% hydrazine hydrate (80 mL). The reaction mixture was stirred at room temperature and refluxed for 24 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure. The resulting residue was recrystallized from ethanol to give 4-hydrazinylpyridin-2(1H)-one as a white solid (yield: 88.3%).TLC detection conditions: dichloromethane/methanol=10/1 (v/v); Rf=0.1.1.1H-NMR (CDCl3) δ: 10.30 (brs, 1H), 7.67 (s, 1H), 7.10 (d, 1H) , 5.79 (d, 1H), 5.54 (s, 1H), 3.91 (brs, 2H). | [References]
[1] Patent: WO2006/25714, 2006, A1. Location in patent: Page/Page column 11
[2] Patent: WO2007/1139, 2007, A1. Location in patent: Page/Page column 15 |
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| Company Name: |
Energy Chemical
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| Tel: |
021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
| Company Name: |
ChemeGen
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| Tel: |
18818260767 |
| Website: |
https://www.chemegen.com |
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