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ChemicalBook >> CAS DataBase List >>D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)-

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)-

CAS No.
1103738-30-2
Chemical Name:
D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)-
Synonyms
SOTA-007;EOS-61382;LX4211 N-4;CPD0854-A1;Sotagliflozin N-4;Intermediates for LX4211;Sotagliflozin Impurity 7;LX4211 N-4 Intermediate 9;(4-Chloro-3-(4-ethoxybenzyl)phenyl)((3aS,5R,6S,6aS);(4-chloro-3-(4-ethoxybenzyl)phenyl)((3aS,5R,6S,6aS)-6-hydroxy-
CBNumber:
CB82667012
Molecular Formula:
C23H25ClO6
Molecular Weight:
432.89
MDL Number:
MFCD25977360
MOL File:
1103738-30-2.mol
MSDS File:
SDS
Last updated:2025-07-24 18:13:41

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- Properties

Boiling point 601.7±55.0 °C(Predicted)
Density 1.271±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
pka 12?+-.0.60(Predicted)
Appearance White to off-white Solid
InChIKey TUBVOYXRJBKZBN-MLNNCEHLSA-N
SMILES O=C(C1=CC=C(Cl)C(CC2=CC=C(OCC)C=C2)=C1)[C@H]1[C@H]([C@H]2[C@@]([H])(O1)OC(O2)(C)C)O

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319
Precautionary statements  P261-P305+P351+P338

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- price More Price(16)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
ChemScene CS-M2124 D-xylo-Pentodialdo-5,2-furanose,1-C-[4-chloro-3-[(4-ethoxyphenyl)methyl]phenyl]-4,5-O-(1-methylethylidene)-,(5S)- 1103738-30-2 250mg $125 2021-12-16 Buy
ChemScene CS-M2124 D-xylo-Pentodialdo-5,2-furanose,1-C-[4-chloro-3-[(4-ethoxyphenyl)methyl]phenyl]-4,5-O-(1-methylethylidene)-,(5S)- 1103738-30-2 1g $250 2021-12-16 Buy
ChemScene CS-M2124 D-xylo-Pentodialdo-5,2-furanose,1-C-[4-chloro-3-[(4-ethoxyphenyl)methyl]phenyl]-4,5-O-(1-methylethylidene)-,(5S)- 1103738-30-2 5g $750 2021-12-16 Buy
ChemScene CS-M2124 D-xylo-Pentodialdo-5,2-furanose,1-C-[4-chloro-3-[(4-ethoxyphenyl)methyl]phenyl]-4,5-O-(1-methylethylidene)-,(5S)- 1103738-30-2 10g $1253 2021-12-16 Buy
Alichem 1103738302 (4-Chloro-3-(4-ethoxybenzyl)phenyl)((3aS,5R,6S,6aS)-6-hydroxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanone 1103738-30-2 10g $1256.1 2021-12-16 Buy
Product number Packaging Price Buy
CS-M2124 250mg $125 Buy
CS-M2124 1g $250 Buy
CS-M2124 5g $750 Buy
CS-M2124 10g $1253 Buy
1103738302 10g $1256.1 Buy

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- Chemical Properties,Uses,Production

Synthesis

4-Bromo-1-chloro-2-(4-ethoxybenzyl)benzene

461432-23-5

((3AS,5R,6S,6aS)-6-hydroxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)(morpholino)methanone

1103738-19-7

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)-

1103738-30-2

Using 4-(2-chloro-5-bromobenzyl)phenyl ethyl ether (Compound C-1, 10 g, 30.7 mmol) and ((3AS,5R,6S,6AS)-6-hydroxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)(morpholino)methanone (Compound B, 9.6 g, 35.3 mmol, 1.15 equivalent) as raw material, the general procedure for the synthesis of (4-chloro-3-(4-ethoxybenzyl)phenyl)((3AS,5R,6S,6AS)-6-hydroxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanone (Compound D-1) was carried out as follows: dissolve Compound C-1 (10 g, 30.7 mmol) in 70 mL of tetrahydrofuran in a 250 mL three-necked flask and stirred until completely dissolved. The solution was cooled to -70 to -80 °C, n-butyllithium solution (2.5 M THF solution, 14.1 mL, 1.15 eq.) was slowly added dropwise and stirred continuously for 1 hour at this temperature. Subsequently, a tetrahydrofuran solution of compound B (9.6 g of B dissolved in 30 mL of tetrahydrofuran) was slowly added dropwise to the reaction mixture. After the dropwise addition was completed, the reaction mixture was continued to be stirred at -70 to -80 °C for 2 hours. After that, the reaction solution was slowly warmed up to -10 to 0 °C and diluted with saturated aqueous NH4Cl solution (20 mL). The reaction mixture was extracted twice with ethyl acetate (100 mL x 2), the organic phases were combined and washed with brine (100 mL). The organic layer was concentrated to dryness under reduced pressure at 40 to 50 °C. The resulting solid was recrystallized by ethyl acetate and hexane to give 11.5 g of compound D-1 in 86.3% yield.

References

[1] Patent: CN108675976, 2018, A. Location in patent: Paragraph 0083; 0084; 0085

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- Preparation Products And Raw materials

Global( 95)Suppliers
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Cangzhou Kangrui Pharma Tech Co. Ltd., 		+86-18632776803 +86-13833998158 cangzhoukangrui@126.com China 751 58
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Jiangxi Huihe Chemical Co., Ltd. 		+86-19189228086 +8618858568638 wuzhouding@huihecrop.com China 886 58
Shanghai Neutan Pharmaceutical Co Ltd 		+undefined15865876430 hujy@neutanpharma.com China 146 58
Zibo Hangyu Biotechnology Development Co., Ltd 		+86-0533-2185556 +8615965530500 nickzhang@hangyubiotech.com China 10985 58

View Lastest Price from D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
(5S)-1-C-[4-Chloro-3-[(4-ethoxyphenyl)methyl]phenyl]-4,5-O-(1-methylethylidene)-D-xylo-pentodialdo-5,2-furanose pictures 2025-07-09 (5S)-1-C-[4-Chloro-3-[(4-ethoxyphenyl)methyl]phenyl]-4,5-O-(1-methylethylidene)-D-xylo-pentodialdo-5,2-furanose
1103738-30-2
 US $0.00-0.00 / g 100g 98% 13kgs Cangzhou Kangrui Pharma Tech Co. Ltd.,
D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- pictures 2019-09-05 D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)-
1103738-30-2
 US $6.00 / KG 1KG 95%-98% 100 Career Henan Chemical Co

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- Spectrum

D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- (4-chloro-3-(4-ethoxybenzyl)phenyl)((3aS,5R,6S,6aS)-6-hydroxy-2,2-diMethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)Methanone (4-chloro-3-(4-ethoxybenzyl)phenyl)((5R,6S)-6-hydroxy-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanone CPD0854-A1 (4-Chloro-3-(4-ethoxybenzyl)phenyl)((3aS,5R,6S,6aS)-6- hydroxy-2,2-dimethyltetrahydrofuro[3,2-d][1,3]dioxol- 5-yl)methanone (5S)-1-C-[4-Chloro-3-[(4-ethoxyphenyl)methyl]phenyl]-4,5-O-(1-methylethylidene)-D-xylo-pentodialdo-5,2-furanose Intermediates for LX4211 LX4211 N-4 Sotagliflozin N-4 SOTA-007 EOS-61382 (4-chloro-3-(4-ethoxybenzyl)phenyl)((3aS,5R,6S,6aS)-6-hydroxy- D-xylo-Pentodialdo-5,2-furanose,1-C-[4-chloro-3-[(4-ethoxyph... TIANFU CHEM D-xylo-Pentodialdo-5,2-furanose, 1-C-[4-chloro-3-[(4-ethoxyphenyl)Methyl]phenyl]-4,5-O-(1-Methylethylidene)-,(5S)- (4-Chloro-3-(4-ethoxybenzyl)phenyl)((3aS,5R,6S,6aS) LX4211 N-4 Intermediate 9 Sotagliflozin Impurity 7 (3-(4-ethoxybenzyl)-4-chlorophenyl)((3aS,5R,6S,6aS)-tetrahydro-6-hydroxy-2,2-dimethylfuro[3,2-d][1,3]dioxol-5-yl)methanone ketone threosee 1103738-30-2