1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
- CAS No.
- 67938-76-5
- Chemical Name:
- 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
- Synonyms
- (5-Chloropyridin-2-yl);5-Chloro-2-pyridinemethanamine;2-Aminomethyl-5-chloropyridine;(5-chloro-2-pyridyl)methanamine;2-Pyridinemethanamine, 5-chloro-;1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE;C-(5-Chloro-pyridin-2-yl)-MethylaMine;2-Aminomethyl-5-chloropyridine hydrochloride;1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE ISO 9001：2015 REACH
- CBNumber:
- CB62454490
- Molecular Formula:
- C6H7ClN2
- Molecular Weight:
- 142.59
- MDL Number:
- MFCD10697658
- MOL File:
- 67938-76-5.mol
- MSDS File:
- SDS
| Boiling point | 216.2±25.0 °C(Predicted) |
|---|---|
| Density | 1.244±0.06 g/cm3(Predicted) |
| storage temp. | under inert gas (nitrogen or Argon) at 2–8 °C |
| solubility | Chloroform (Slightly), Methanol (Slightly) |
| pka | 8.31±0.39(Predicted) |
| form | Low-Melting Solid |
| color | Pale Yellow to Light Yellow |
1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE price More Price(15)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | C596263 | (5-Chloropyridin-2-yl)methanamine | 67938-76-5 | 25mg | $45 | 2021-12-16 | Buy |
| TRC | C596263 | (5-Chloropyridin-2-yl)methanamine | 67938-76-5 | 50mg | $60 | 2021-12-16 | Buy |
| TRC | C596263 | (5-Chloropyridin-2-yl)methanamine | 67938-76-5 | 250mg | $75 | 2021-12-16 | Buy |
| AK Scientific | 7855BB | (5-Chloropyridin-2-YL)methanamine | 67938-76-5 | 1g | $208 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0064047 | (5-CHLOROPYRIDIN-2-YL)METHANAMINE 95.00% | 67938-76-5 | 5G | $2752.94 | 2021-12-16 | Buy |
1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Chemical Properties,Uses,Production
Synthesis
89809-64-3
67938-76-5
The general procedure for the synthesis of 2-aminomethyl-5-chloropyridine from 5-chloro-2-cyanopyridine was as follows: 5-chloropyridinecarbonitrile (3.8 g, 27.43 mmol) was dissolved in ethanol (100 mL), and concentrated HCl (3 mL) and 10% Pd-C catalyst (1.0 g) were added. The reaction mixture was shaken under hydrogen atmosphere (40 psi) for 2 hours. After completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated. The obtained residue was dissolved in saturated NaHCO3 solution (50 mL) and extracted with dichloromethane (4 x 25 mL). The organic phases were combined, dried with anhydrous Na2SO4, filtered and concentrated to afford 2-aminomethyl-5-chloropyridine as a yellow oil (2.0 g, 51% yield). The product was analyzed by LCMS showing a (M + H)+ peak of 143.07 (calculated value: 143.04, C6H8ClN2).1HNMR (500 MHz, CDCl3) δ ppm: 8.56-8.51 (1H, br d), 7.66-7.60 (1H, m), 7.28-7.14 (1H, m), 3.97 (2H. s), 1.72 (2H, s).
References
[1] Patent: US2005/267105, 2005, A1. Location in patent: Page/Page column 63
[2] Patent: US2007/111984, 2007, A1. Location in patent: Page/Page column 29
[3] Patent: US2007/129379, 2007, A1. Location in patent: Page/Page column 21-22
[4] Patent: WO2007/64316, 2007, A1. Location in patent: Page/Page column 140 - 141
1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Hubei xin bonus chemical co. LTD | 86-13657291602 | linda@hubeijusheng.com | CHINA | 22963 | 58 |
| Shandong chuangyingchemical Co., Ltd. | 18853181302 | sale@chuangyingchem.com | CHINA | 5906 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49733 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29804 | 58 |
| Fuxin Pharmaceutical | +86-021-021-50872116 +8613122107989 | contact@fuxinpharm.com | China | 10035 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
| ANHUI WITOP BIOTECH CO., LTD | +8615255079626 | eric@witopchemical.com | China | 23541 | 58 |
| Dideu Industries Group Limited | +86-29-89586680 +86-15129568250 | 1026@dideu.com | China | 21993 | 58 |
| Hefei Hirisun Pharmatech Co., Ltd | +8615056975894 | shawn@hirisunpharm.com | CHINA | 9911 | 58 |
| CR Corporation Limited | +8613062833949 | fred.wen@crcorporation.cn | China | 8647 | 58 |
View Lastest Price from 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2021-09-04 | 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
67938-76-5
|
US $1.10 / g | 1g | 99.00% | 100 Tons min | Dideu Industries Group Limited | |
 |
2020-02-19 | 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
67938-76-5
|
US $7.00 / KG | 1KG | 99% | 100kg | Career Henan Chemical Co |
-
- 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
67938-76-5
- US $1.10 / g
- 99.00%
- Dideu Industries Group Limited
-
- 1-(5-CHLOROPYRIDIN-2-YL)METHANAMINE
67938-76-5
- US $7.00 / KG
- 99%
- Career Henan Chemical Co
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