(6-CHLORO-5-METHYLPYRIDIN-3-YL)METHANOL
- CAS No.
- 887707-21-3
- Chemical Name:
- (6-CHLORO-5-METHYLPYRIDIN-3-YL)METHANOL
- Synonyms
- 6-chloro-5-methyl-3-Pyridinemethanol;3-Pyridinemethanol, 6-chloro-5-methyl-;(6-CHLORO-5-METHYLPYRIDIN-3-YL)METHANOL;2-Chloro-5-hydroxymethyl-3-methylpyridine
- CBNumber:
- CB52449354
- Molecular Formula:
- C7H8ClNO
- Molecular Weight:
- 157.6
- MDL Number:
- MFCD09261083
- MOL File:
- 887707-21-3.mol
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H320-H335 |
| Precautionary statements | P261-P280-P301+P312-P302+P352-P305+P351+P338 |
| HS Code | 2933399990 |
(6-CHLORO-5-METHYLPYRIDIN-3-YL)METHANOL price More Price(30)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | C993360 | (6-Chloro-5-methylpyridin-3-yl)methanol | 887707-21-3 | 500mg | $265 | 2021-12-16 | Buy |
| Apolloscientific | OR310307 | (6-Chloro-5-methylpyridin-3-yl)methanol | 887707-21-3 | 1g | $290 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC143563 | (6-Chloro-5-methylpyridin-3-yl)methanol | 887707-21-3 | 100mg | $125 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC143563 | (6-Chloro-5-methylpyridin-3-yl)methanol | 887707-21-3 | 250mg | $200 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FC143563 | (6-Chloro-5-methylpyridin-3-yl)methanol | 887707-21-3 | 500mg | $300 | 2021-12-16 | Buy |
(6-CHLORO-5-METHYLPYRIDIN-3-YL)METHANOL Chemical Properties,Uses,Production
Synthesis
176433-43-5
887707-21-3
To a solution of 6-chloro-5-methylnicotinaldehyde (3.20 g, 20.7 mmol) in methanol (22 mL) was slowly added sodium borohydride (863 mg, 22.7 mmol) at 0 °C. The reaction mixture was stirred at room temperature for 2 hours. Subsequently, saturated aqueous ammonium chloride solution (20 mL) was added and the mixture continued to be stirred for 0.5 hours. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was washed with water (50 mL) and extracted with dichloromethane (50 mL x 3). The organic layers were combined, dried over anhydrous sodium sulfate and concentrated. The resulting residue was purified by silica gel column chromatography (eluent ratio of petroleum ether/ethyl acetate=2/1) to afford the target product (6-chloro-5-methylpyridin-3-yl)methanol (3.2 g, 88% yield) as a light yellow solid.1H NMR (400 MHz, CDCl3) δ 8.09 (s, 1H), 7.56 (s, 1H), 4.65 (s 2H), 2.33 (s, 3H).
References
[1] European Journal of Medicinal Chemistry, 2016, vol. 108, p. 154 - 165
[2] Patent: WO2006/114213, 2006, A1. Location in patent: Page/Page column 30
(6-CHLORO-5-METHYLPYRIDIN-3-YL)METHANOL Preparation Products And Raw materials
(6-CHLORO-5-METHYLPYRIDIN-3-YL)METHANOL Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
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