3-(Boc-amino)-3-methylpip...
- CAS No.
- 169750-96-3
- Chemical Name:
- 3-(Boc-amino)-3-methylpip...
- Synonyms
- 3-(Boc-amino)-3-methylpip...;3-(Boc-aMino)-3-Methylpiperidine;3-Amino-3-methylpiperidine, 3-BOC protected;tert-Butyl 3-methylpiperidin-3-yl-carbamate;tert-butyl n-(3-methylpiperidin-3-yl)carbamate;(3-Methyl-piperidin-3-yl)-carbamic acid tert-butyl ester;(3-Methyl-3-piperidinyl)carbamic acid 1,1-dimethylethyl ester;Carbamic acid, N-(3-methyl-3-piperidinyl)-, 1,1-dimethylethyl ester;tert-Butyl (3-methylpiperidin-3-yl)carbamate, 3-[(tert-Butoxycarbonyl)amino]-3-methylpiperidine
- CBNumber:
- CB22525095
- Molecular Formula:
- C11H22N2O2
- Molecular Weight:
- 214.3
- MDL Number:
- MFCD13194151
- MOL File:
- 169750-96-3.mol
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H302-H315-H319-H335 |
Precautionary statements | P261-P305+P351+P338 |
HS Code | 2933399990 |
3-(Boc-amino)-3-methylpip... price More Price(13)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
TRC | B630050 | 3-(Boc-amino)-3-methylpiperidine | 169750-96-3 | 100mg | $75 | 2021-12-16 | Buy |
AK Scientific | Y1662 | 3-(Boc-amino)-3-methylpiperidine | 169750-96-3 | 1g | $167 | 2021-12-16 | Buy |
AK Scientific | Y1662 | 3-(Boc-amino)-3-methylpiperidine | 169750-96-3 | 5g | $402 | 2021-12-16 | Buy |
American Custom Chemicals Corporation | CHM1052023 | TERT-BUTYL N-(3-METHYLPIPERIDIN-3-YL)CARBAMATE 95.00% | 169750-96-3 | 5MG | $450.59 | 2021-12-16 | Buy |
SynQuest Laboratories | 4H51-1-2V | 3-Amino-3-methylpiperidine, 3-Boc protected | 169750-96-3 | 1g | $525 | 2021-12-16 | Buy |
3-(Boc-amino)-3-methylpip... Chemical Properties,Uses,Production
Synthesis
![1-Piperidinecarboxylic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-3-methyl-, phenylmethyl ester](/CAS/20210111/GIF/1196506-86-1.gif)
1196506-86-1

169750-96-3
General procedure for the synthesis of tert-butyl (3-methylpiperidin-3-yl)carbamate from the compound (CAS:1196506-86-1): benzyl 3-((tert-butoxycarbonyl)amino)-3-methylpiperidine-1-carboxylate (78 mg, 0.22 mmol, prepared according to the method described in WO09/140320) was dissolved in EtOH (5 mL) , which was degassed by bubbling N2 (g) into the solution for 10 min. Pd/C (10 wt%, 24 mg, 0.022 mmol) was added. A gas bladder attached to a three-way cork filled with H2 was connected to the flask. The flask was evacuated and backfilled with H2 (repeated 3 times). The mixture was stirred at room temperature for 2 hours. Degassing was again carried out by bubbling N2 (g) into the solution for 10 min, followed by filtration through diatomaceous earth. The filtrate was concentrated to give racemic-tert-butyl (3-methylpiperidin-3-yl) carbamate (42 mg, 0.20 mmol, 88% yield) as a clear, colorless oil.MS (ESI, cationic) m/z: 215.1 (M + 1).
References
[1] Patent: WO2012/148775, 2012, A1. Location in patent: Page/Page column 124; 125
[2] Patent: WO2009/140320, 2009, A1. Location in patent: Page/Page column 73
3-(Boc-amino)-3-methylpip... Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Hi-Tech Chemistry Corp | 0519-86626038 | yuhh@hitechem.com | CHINA | 810 | 58 |
career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29804 | 58 |
Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
Blocksynth Pharmaceutical Technology Co.,Ltd | 0086-19817745290; +8619817745290 | bd@blocksynth.com | China | 5661 | 58 |
Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52846 | 58 |
CR Corporation Limited | +8613062833949 | fred.wen@crcorporation.cn | China | 8647 | 58 |
Henan Alfa Chemical Co., Ltd | +8615838112936 | alfa10@alfachem.cn | China | 12949 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25356 | 58 |
PT CHEM GROUP LIMITED | +86-85511178; | peter68@ptchemgroup.com | China | 35425 | 58 |
GIHI CHEMICALS CO.,LIMITED | +8618058761490 | info@gihichemicals.com | China | 49983 | 58 |
View Lastest Price from 3-(Boc-amino)-3-methylpip... manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
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2020-01-10 | tert-butyl (3-methylpiperidin-3-yl)carbamate
169750-96-3
|
US $1.00 / KG | 1KG | 99% | 200kg | Career Henan Chemical Co |
-
- tert-butyl (3-methylpiperidin-3-yl)carbamate
169750-96-3
- US $1.00 / KG
- 99%
- Career Henan Chemical Co