Methyl 2-bromo-6-fluorobenzoate
- CAS No.
- 820236-81-5
- Chemical Name:
- Methyl 2-bromo-6-fluorobenzoate
- Synonyms
- Methyl 2-bromo-6-fluorobenzoate;Benzoic acid, 2-bromo-6-fluoro-, methyl ester
- CBNumber:
- CB02513584
- Molecular Formula:
- C8H6BrFO2
- Molecular Weight:
- 233.03
- MDL Number:
- MFCD10000922
- MOL File:
- 820236-81-5.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P280-P302+P352-P304+P340 |
| HS Code | 2916399090 |
Methyl 2-bromo-6-fluorobenzoate price More Price(25)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | M295920 | Methyl2-bromo-6-fluorobenzoate | 820236-81-5 | 100mg | $45 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FB70039 | 2-Bromo-6-fluorobenzoic acid methyl ester | 820236-81-5 | 10g | $60 | 2021-12-16 | Buy |
| SynQuest Laboratories | 2723-B-01 | Methyl 2-bromo-6-fluorobenzoate | 820236-81-5 | 1g | $61 | 2021-12-16 | Buy |
| AK Scientific | Z0862 | 2-Bromo-6-fluorobenzoicacidmethylester | 820236-81-5 | 1g | $70 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FB70039 | 2-Bromo-6-fluorobenzoic acid methyl ester | 820236-81-5 | 25g | $100 | 2021-12-16 | Buy |
Methyl 2-bromo-6-fluorobenzoate Chemical Properties,Uses,Production
Synthesis
67-56-1
2252-37-1
820236-81-5
Step 1: Synthesis of methyl 2-bromo-6-fluorobenzoate (2). 2-Bromo-6-fluorobenzoic acid (1, 12.50 g, 57 mmol) was dissolved in a mixture of methanol (60 mL) and concentrated sulfuric acid (65 mL). The reaction mixture was heated to 80 °C and stirred at this temperature for 12 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the pH was adjusted slowly by adding 20% sodium carbonate solution (500 mL) to 8. Subsequently, extraction was carried out with dichloromethane (3 x 180 mL), the organic phases were combined and dried with anhydrous magnesium sulfate. Finally, the solvent was evaporated under reduced pressure to afford the title compound methyl 2-bromo-6-fluorobenzoate (11.29 g, 48.5 mmol, 85% yield) as a brown oil.
References
[1] Patent: WO2011/156786, 2011, A2. Location in patent: Page/Page column 128
[2] Patent: WO2013/86451, 2013, A2. Location in patent: Paragraph 00499
[3] Bioorganic and Medicinal Chemistry Letters, 2015, vol. 25, # 20, p. 4393 - 4398
Methyl 2-bromo-6-fluorobenzoate Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 | info@spring-chem.com | China | 2068 | 57 |
| Capot Chemical Co.,Ltd. | +8613336195806 | sales@capot.com | China | 29731 | 60 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29804 | 58 |
| Fuxin Pharmaceutical | +86-021-021-50872116 +8613122107989 | contact@fuxinpharm.com | China | 10035 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | sales@win-winchemical.com | China | 14459 | 58 |
| CD Chemical Group Limited | +8615986615575 | info@codchem.com | China | 20342 | 58 |
| Changzhou Anxuan Chemical Co., Ltd | +86-0519-89882563 +86-18961279162 | andy@anxuanchem.com | China | 4327 | 58 |
| Nanjing Hengbei Chemicals Co., Ltd. | +86-25-58393656 | sales@hengbeichem.cn | China | 6854 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418684 +8618949823763 | sales@tnjchem.com | China | 25356 | 58 |
View Lastest Price from Methyl 2-bromo-6-fluorobenzoate manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-08 | Methyl 2-bromo-6-fluorobenzoate
820236-81-5
|
US $1.00 / KG | 1KG | 99% | 100KG | Career Henan Chemical Co |
-
- Methyl 2-bromo-6-fluorobenzoate
820236-81-5
- US $1.00 / KG
- 99%
- Career Henan Chemical Co
