| Identification | Back Directory | [Name]
1-Methylcyclopropylamine hydrochloride | [CAS]
88887-87-0 | [Synonyms]
1-Methylcyclopropanamine HCl
1-methylcyclopropaneamine HCl
1-Methylcyclopropanaminium chloride
1-Methylcyclopropylamine hydrochloride
1-MethylcyclopropanaMine hydrochloride
1-Methylcyclopropan-1-amine hydrochloride
1-aMino-1-Methylcyclopropane hydrochloride
1-methylcyclopropanamine hydrochloride (1:1)
1-Methylcyclopropan-1-amine hydrochloride 98%
CyclopropanaMine,1-Methyl-, hydrochloride (1:1)
(1-Methylcyclopropyl)aMine hydrochloride (SALTDATA: HCl) | [Molecular Formula]
C4H10ClN | [MDL Number]
MFCD11109576 | [MOL File]
88887-87-0.mol | [Molecular Weight]
107.582 |
| Hazard Information | Back Directory | [Synthesis]
(2) N-Boc-1-methylcyclopropylamine (4.66 g) obtained in step (1) was dissolved in 1,4-dioxane (10 mL), followed by addition of a 4N hydrochloric acid solution of dioxane (10 mL). The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, diisopropyl ether was added to the mixture and the precipitated crystals were collected by filtration to afford 1-methylcyclopropanamine hydrochloride (2.69 g, yield: 92%) as a colorless solid. Mass spectrum (APCI) m/z: 72 [M+H]+. | [References]
[1] Patent: WO2008/4698, 2008, A2. Location in patent: Page/Page column 129
[2] Patent: WO2011/6074, 2011, A1. Location in patent: Page/Page column 127
[3] Patent: WO2006/67444, 2006, A1. Location in patent: Page/Page column 84-85
[4] Patent: WO2005/42502, 2005, A1. Location in patent: Page/Page column 81-82 |
|
|