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ChemicalBook--->CAS DataBase List--->76006-17-2

76006-17-2

76006-17-2 Structure

76006-17-2 Structure
IdentificationBack Directory
[Name]

1H-PYRAZOLO[3,4-C]PYRIDIN-3-AMINE
[CAS]

76006-17-2
[Synonyms]

4-c]pyridin-3-aMine
3-Amino-6-aza-1H-indazole
1H-PYRAZOLO[3,4-C]PYRIDIN-3-AMINE
3-Amino-1H-pyrazolo[3,4-c]pyridine
1H-Pyrazolo[3,4-c]pyridin-3-ylamine
3-Amino-1H-pyrazolo[3,4-c]pyridine 95+%
1H-Pyrazolo[3,4-c]pyridin-3-amine, 3-Amino-6-azaindole
[Molecular Formula]

C6H6N4
[MDL Number]

MFCD11656373
[MOL File]

76006-17-2.mol
[Molecular Weight]

134.14
Chemical PropertiesBack Directory
[Melting point ]

213-214 °C(Solv: ethanol (64-17-5))
[Boiling point ]

433.5±25.0 °C(Predicted)
[density ]

1.480±0.06 g/cm3(Predicted)
[storage temp. ]

2-8°C(protect from light)
[form ]

solid
[pka]

11.83±0.40(Predicted)
[Appearance]

White to yellow Solid
Safety DataBack Directory
[Symbol(GHS) ]


GHS06
[Signal word ]

Danger
[Hazard statements ]

H301-H319
[Precautionary statements ]

P301+P310-P305+P351+P338
[Hazard Codes ]

T
[Risk Statements ]

25-36
[Safety Statements ]

26-45
[RIDADR ]

UN 2811 6.1 / PGIII
[HS Code ]

2933399990
Spectrum DetailBack Directory
[Spectrum Detail]

1H-PYRAZOLO[3,4-C]PYRIDIN-3-AMINE(76006-17-2)1HNMR
Hazard InformationBack Directory
[Synthesis]

3-Fluoropyridine-4-carbonitrile

113770-88-0

1H-PYRAZOLO[3,4-C]PYRIDIN-3-AMINE

76006-17-2

General procedure for the synthesis of 1H-pyrazolo[3,4-c]pyridin-3-amine using 3-fluoro-4-cyanopyridine as starting material: 3-fluoro-4-cyanopyridine (0.50 g, 4.10 mmol) was dissolved in ethanol (8 mL), followed by addition of hydrazine hydrate (0.31 g, 6.1 mmol). The reaction mixture was stirred at 70 °C for 16 hours. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated and dried under vacuum to afford the target product 1H-pyrazolo[3,4-c]pyridin-3-amine (0.66 g, 100% yield). The product was characterized by LC-MS (Method 2B): retention time (Rt) = 0.51 min, mass spectrum (ESI positive ion mode): m/z = 135 [M + H]+.

[References]

[1] Patent: WO2015/67549, 2015, A1. Location in patent: Page/Page column 66
[2] Patent: US2015/126449, 2015, A1. Location in patent: Paragraph 0386 - 0388
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