| Identification | Back Directory | [Name]
1,3-Dichloro-2,2-dimethoxypropane | [CAS]
6626-57-9 | [Synonyms]
1,3-DICHLORO-2,2-DIMETHOXY-PROPANE
Propane, 1,3-dichloro-2,2-dimethoxy-
1,3-DICHLORO-2,2-DIMETHOXY-PROPANE 98% | [Molecular Formula]
C5H10Cl2O2 | [MDL Number]
MFCD00130264 | [MOL File]
6626-57-9.mol | [Molecular Weight]
173.04 |
| Chemical Properties | Back Directory | [Melting point ]
81.5 °C | [Boiling point ]
194.0±35.0 °C(Predicted) | [density ]
1.180±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,Room Temperature | [Appearance]
White to off-white Solid |
| Hazard Information | Back Directory | [Synthesis]
In a 150 mL three-neck flask, 17.42 g of acetone and 43.55 g of methanol were added, the reaction temperature was controlled in the range of 20-35 °C, and chlorine gas was slowly passed through. When the chlorine gas was passed in an amount of about 42.0 g, the chlorine gas was stopped and the reaction mixture was continued to be stirred for 0.5 hours. Subsequently, the reaction mixture was cooled to 0-5 °C, and filtration was carried out to afford 42.24 g of 1,3-dichloro-2,2-dimethoxypropane in 81.2% yield. | [References]
[1] Patent: CN105461529, 2016, A. Location in patent: Paragraph 0012; 0020 |
|
| Company Name: |
Struchem Co., Ltd.
|
| Tel: |
0512-63009836 18994340901 |
| Website: |
www.beidapharma.com |
| Company Name: |
Cool Pharm, Ltd
|
| Tel: |
021-58581007 18019463053 |
| Website: |
www.coolpharm.com.cn |
|