| Identification | Back Directory | [Name]
7-BROMO-2-METHYLQUINAZOLINE | [CAS]
552331-87-0 | [Synonyms]
7-BROMO-2-METHYLQUINAZOLINE
Quinazoline, 7-bromo-2-methyl- | [Molecular Formula]
C9H7BrN2 | [MDL Number]
MFCD11044811 | [MOL File]
552331-87-0.mol | [Molecular Weight]
223.07 |
| Chemical Properties | Back Directory | [Boiling point ]
244.8±22.0 °C(Predicted) | [density ]
1.565±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,Room Temperature | [pka]
4.24±0.70(Predicted) | [Appearance]
Off-white to light yellow Solid |
| Hazard Information | Back Directory | [Synthesis]
Example 239A Synthesis of 7-bromo-2-methylquinazoline: 4-bromo-2-fluorobenzaldehyde (1 g, 4.9 mmol), acetamidine, and N,N-dimethylacetamide (DMA) were mixed, heated to 140°C, and reacted for 5 hours. After completion of the reaction, the mixture was cooled to room temperature and dried under vacuum. The crude product was purified by fast column chromatography to give 47 mg of the target compound in 4% yield. The mass spectrum (ESI) m/e 223 (M + 1)+. | [References]
[1] Patent: US2003/187026, 2003, A1
[2] Patent: US2003/199511, 2003, A1. Location in patent: Page/Page column 72 |
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China Langchem Inc.
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SynAsst Chemical.
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Cool Pharm, Ltd
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