| Identification | Back Directory | [Name]
2-Methylaminopyridine-3-carbaldehyde | [CAS]
32399-08-9 | [Synonyms]
2-(Methylamino)nicotinaldehyde
2-Methylaminopyridine-3-carbaldehyde
2-Methylamino-3-pyridinecarboxaldehyde
3-Pyridinecarboxaldehyde, 2-(methylamino)-
2-(methylamino)nicotinaldehyde(SALTDATA: HCl) | [Molecular Formula]
C7H8N2O | [MDL Number]
MFCD05863669 | [MOL File]
32399-08-9.mol | [Molecular Weight]
136.15 |
| Chemical Properties | Back Directory | [Boiling point ]
281.7±25.0 °C(Predicted) | [density ]
1.196±0.06 g/cm3(Predicted) | [storage temp. ]
under inert gas (nitrogen or Argon) at 2-8°C | [pka]
5.00±0.10(Predicted) | [Appearance]
Light yellow to brown Liquid |
| Hazard Information | Back Directory | [Synthesis]
Preparation of 2-(Methylamino)nicotinaldehyde: 9.10 g (66.0 mmol) of 2-(methylamino)-3-pyridinemethanol was dissolved in 70 mL of chloroform and 17.4 g (200 mmol) of manganese dioxide was added. The reaction mixture was stirred at 60 °C overnight. Upon completion of the reaction, the mixture was filtered and the filtrate was concentrated to give 8.66 g (yield: 96%) of 2-(methylamino)nicotinaldehyde as an orange solid.NMR data (CDCl3/TMS, δ, ppm): 3.10 (3H, d), 6.62-6.66 (1H, m), 7.74 (1H, d), 8.36 (1H, d), 9.80 (1H, s). | [References]
[1] Patent: US2011/287937, 2011, A1. Location in patent: Page/Page column 69 |
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| Company Name: |
Tetranov Biopharm
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| Tel: |
13526569071 |
| Website: |
http://www.leadmedpharm.com/index.html |
| Company Name: |
Wuxi AppTec
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| Tel: |
022-59987777 13552403979 |
| Website: |
www.labnetwork.com |
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