Identification | Back Directory | [Name]
2,6-DICHLOROIMIDAZO[1,2-B]PYRIDAZINE | [CAS]
112581-77-8 | [Synonyms]
2,6-DICHLOROIMIDAZO[1,2-B]PYRIDAZINE IMidazo[1,2-b]pyridazine,2,6-dichloro- 2,6-DICHLOROIMIDAZO[1,2-B]PYRIDAZINE ISO 9001:2015 REACH | [Molecular Formula]
C6H3Cl2N3 | [MDL Number]
MFCD11044765 | [MOL File]
112581-77-8.mol | [Molecular Weight]
188.01 |
Chemical Properties | Back Directory | [density ]
1.69 | [storage temp. ]
2-8°C | [InChI]
InChI=1S/C6H3Cl2N3/c7-4-1-2-6-9-5(8)3-11(6)10-4/h1-3H | [InChIKey]
MGNCSIAIZSTMHX-UHFFFAOYSA-N | [SMILES]
C12=NC(Cl)=CN1N=C(Cl)C=C2 |
Hazard Information | Back Directory | [Synthesis]
Example 4: 1.88 g of 6-chloro-3-imino-2,3-dihydropyridazine-2-acetic acid (purity: 99.5 wt%) was mixed with 7.52 g of monochlorobenzene and 0.79 g of pyridine. 3.84 g of phosphoryl chloride was slowly added dropwise to the mixture over a period of 3 minutes at an endothermic condition of 20 to 40 °C. Subsequently, the reaction system was heated to an endothermic temperature of 120 °C within 20 minutes and the reaction was continued at this temperature for 6 hours. Upon completion of the reaction, the mixture was cooled to give a reaction mixture containing 2,6-dichloroimidazo[1,2-b]pyridazine.The yield of 2,6-dichloroimidazo[1,2-b]pyridazine was 99%. | [References]
[1] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 5 [2] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 4 [3] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 4 [4] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 5 [5] Patent: EP1930331, 2008, A1. Location in patent: Page/Page column 5 |
|
Company Name: |
Heterochem
|
Tel: |
027-88041443 13072715837 |
Website: |
www.hetero-chem.com |
|